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Home > Chemical Processing > Chemical Processing > MP1010

Continuous distillation


Service : 230 V / 50 Hz / Single phase: 4 kW.
Cold water 20 C / 3 bar: 1 m3 / h. Sewer.
Dimensions : 1,55 m x 0,65 m x 3,05 m
Weight : 180kg

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DEMANDER UN DEVIS POUR CETTE MACHINE



Principle of operation :

Distillation allows the separation of a mixture of compounds having different boiling points. The boiling of the mixture makes it possible to obtain vapors of compositions different from the liquid. Re-condensations and multiple re-evaporations progressively enrich the vapor phase to the most volatile product. The vapors are condensed and then distributed between the distillate and the reflux via a column head valve.




Educational Objectives :

Educational goals : 

  • Study of the hydrodynamics of the column.
  • Influence of the operating conditions on the separation of a binary solution
  • Thermal balances.
  • Material balance.
  • Determination of the number of theoretical plates (McCabe and Thiele, Ponchon and Savart).
  • Determination of the number of transfer units
Technical specifications :
  • Storage can of the polyethylene feed solution.
  • Feeder dosing pump.
  • Preheater with two valves for supply at 33% or 66% of the column,
  • Continuous boiler in borosilicate glass, electric heating, equipped with minimum safety level and maximum temperature safety.
  • Refrigerant for differential pressure test.
  • Column in borosilicate glass, in three elements with lining.
  • Three stainless steel 316L recentering trays, each equipped with sampling and temperature sampling valve.
  • Borosilicate glass column head, with temperature measurement, equipped with a timer valve to control the reflux ratio.
  • Vertical 316L stainless steel condenser, borosilicate glass ferrule.
  • Two refrigerants of distillate and residue in 316L stainless steel.
  • Recipe for borosilicate glass distillate.
  • Recipe of the borosilicate glass residue, equipped with a 316L stainless steel drain valve.
  • Two containers for receiving the distillate and the polyethylene residue
  • 316L stainless steel connection pipes.
  • Support frame in 304L stainless steel tubes and aluminum nuts.


Instrumentation :

  • Condenser cooling water supply equipped with a float flowmeter with its control valve and a water circulation controller to stop heating due to lack of cooling.
  • Column pressure drop measurement using a "U" differential pressure gauge.
  • Control and control cabinet, IP55, equipped with emergency stop, operating buttons and the following interfaces:
  • Preheater temperature controller.
  • Electronic timer controlling the valve of the column head.
  • Boiler heating control regulator.
  • Two digital temperature indicators of 12 probes type Pt100 Ω.
Options :
Touch screen to view temperatures and control the regulators. With data storage and data recovery on USB stick in .txt files.
DEMANDER UN DEVIS POUR CETTE MACHINE

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