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Home > Chemical Processing > Chemical Processing > MP1070

Reacted reactor 10 liters


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Service : 230 V / 50 Hz / Single phase: 1 kW.
Cold water 20 ° C / 3 bar: 1 m3 / h.
Empty 100 mbar: 2 Nm3 / h
Steam 4 bar: 5 kg / h.
Sewer for heating condensates.
Dimensions : 1,90 m x 0,83 m x 3,05 m
Weight : ~ 250 kg

Print / download the product sheet
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Principle of operation
 

The reaction is a fundamental operation of the chemical industry, making it possible to produce, from simple molecules (reagents), more and more complex compounds intended for a growing number of industries (chemistry, pharmacy, etc.).
The reactor is of the perfectly stirred type and operates discontinuously: the quantity of reagent is introduced at the beginning of the handling at one time or controlled as a function of time. The reactor also makes it possible to make "batch" crystallizations.




Educational Objectives :
  • Study of simple reactions.
  • Study of kinetics of reaction.
  • Study of reversible or irreversible reactions.
  • Study of evaporation.
  • Crystallization by evaporation, chemical reaction or cooling.
  • Total reflux reactions.
  • Discontinuous distillation.
  • Material balance.
  • Conversion rate.
  • Thermal balance.
Technical specifications :

Technical specifications.
 


Equipment
 

  • Storage reagent recipe in borosilicate glass, graduated with "juice elevator" system for filling reagents.
  • Cylindrical reactor type "GRIGNARD": with double steam heating jacket, flush drain valve and operator protection; borosilicate glass lid.
  • 316L stainless steel variable speed stirring unit with inclined tri-blade impeller.
  • Cooling coil of the 316L stainless steel reaction mass.
  • Column in borosilicate glass, in one element with 316L stainless steel lining.
  •  Borosilicate glass column head, with temperature measurement, equipped with a timer valve to control the reflux ratio.
  •  Vertical 316L stainless steel condenser, borosilicate glass ferrule.
  •  316L stainless steel distillate coolant.
  •  Recipes of borosilicate glass distillate, graduated.
  •  Circuit for relaxing and adjusting the heating steam with operator protection panel.
  •  Heating hoses for insulated heating steam.
  •  316L stainless steel connection pipes.
  •  Support frame in 304L stainless steel tubes and aluminum nuts.

     

Instrumentation
 

  • Condenser cooling water supply equipped with a float flowmeter with its control valve and a water circulation controller to stop heating due to lack of cooling.
  • Measurement of supply pressure of the heating vapor by manometer.
  • Control and control cabinet, IP55, equipped with emergency stop, operating buttons and the following interfaces:
  • Electronic timer controlling the valve of the column head.
  • Regulator of the temperature of the reactor.
  • Variator of the stirring speed.
  • Digital indicator of stirring speed.
  • Two digital temperature indicators of five Pt100 Ω probes.
Options :
Option 1: Reduced pressure bag filter in 316L stainless steel; capacity 9 liters (cake) + 9 liters (filtrate)
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