
Non contractual photo
Service : 230 V / 50 Hz / Single phase: 1 kW.
Cold water 20 ° C / 3 bar: 1 m3 / h.
Empty 100 mbar: 2 Nm3 / h
Steam 4 bar: 5 kg / h.
Sewer for heating condensates.
Dimensions : 1,90 m x 0,83 m x 3,05 m
Weight : ~ 250 kg
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Principle of operation
The reaction is a fundamental operation of the chemical industry, making it possible to produce, from simple molecules (reagents), more and more complex compounds intended for a growing number of industries (chemistry, pharmacy, etc.).
The reactor is of the perfectly stirred type and operates discontinuously: the quantity of reagent is introduced at the beginning of the handling at one time or controlled as a function of time. The reactor also makes it possible to make "batch" crystallizations.
Technical specifications.
Equipment
- Storage reagent recipe in borosilicate glass, graduated with "juice elevator" system for filling reagents.
- Cylindrical reactor type "GRIGNARD": with double steam heating jacket, flush drain valve and operator protection; borosilicate glass lid.
- 316L stainless steel variable speed stirring unit with inclined tri-blade impeller.
- Cooling coil of the 316L stainless steel reaction mass.
- Column in borosilicate glass, in one element with 316L stainless steel lining.
- Borosilicate glass column head, with temperature measurement, equipped with a timer valve to control the reflux ratio.
- Vertical 316L stainless steel condenser, borosilicate glass ferrule.
- 316L stainless steel distillate coolant.
- Recipes of borosilicate glass distillate, graduated.
- Circuit for relaxing and adjusting the heating steam with operator protection panel.
- Heating hoses for insulated heating steam.
- 316L stainless steel connection pipes.
- Support frame in 304L stainless steel tubes and aluminum nuts.
Instrumentation
- Condenser cooling water supply equipped with a float flowmeter with its control valve and a water circulation controller to stop heating due to lack of cooling.
- Measurement of supply pressure of the heating vapor by manometer.
- Control and control cabinet, IP55, equipped with emergency stop, operating buttons and the following interfaces:
- Electronic timer controlling the valve of the column head.
- Regulator of the temperature of the reactor.
- Variator of the stirring speed.
- Digital indicator of stirring speed.
- Two digital temperature indicators of five Pt100 Ω probes.
Option 1: Reduced pressure bag filter in 316L stainless steel; capacity 9 liters (cake) + 9 liters (filtrate)