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Home > Chemical Processing > Chemical Processing > MP1075

Versatile synthesis unit 50 liters


Service : 400 V / 50 Hz / Three phase + N: 1 kW.
Cold water 20 C / 3 bar: 1 m3 / h.
Empty 20 mbar: 60 Nm3 / h
Steam 6 bar: 30 kg / h.
Sewer for heating condensates.
Dimensions : 2, 50 m x 1, 04 m x 3, 65 m
Weight : ~ 600 kg

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DEMANDER UN DEVIS POUR CETTE MACHINE

Principle of operation

The reaction is a fundamental operation of the chemical industry, making it possible to produce, from simple molecules (reagents), more and more complex compounds intended for a growing number of industries (chemistry, pharmacy, etc.).




Educational Objectives :
  • Study of simple reactions.
  • Study of evaporation.
  • Crystallization by evaporation, chemical reaction or cooling.
  • Total reflux reactions.
  • Discontinuous distillation.
  • Discontinuous heteroazeotrope distillation.
  • Discontinuous distillation under reduced pressure.
  • Material balance.
  • Yields.
  • Thermal balance.
Technical specifications :

Equipment
 

  •     Storage reagent recipe in borosilicate glass, graduated with "juice elevator" system for filling reagents.
  •     Frustoconical reactor: 316L stainless steel tank, double steam heating jacket, flush drain valve, operator protection panel, 316L stainless steel cover.
  •     Fixed speed stirring set in 316L stainless steel with "V" anchor.
  •     316L stainless steel column, DN100, in a 1200 mm element with "MULTIKNIT" type 316L stainless steel lining.
  •     Inclined multitubular condenser.
  •     Decanter in borosilicate glass, cooled, with manual adjustment of the level of the interface.
  •     Recipes of borosilicate glass distillate, graduated.
  •     Circuit for relaxing and adjusting the heating steam with operator protection panel.
  •     316L stainless steel piping.
  •     316L stainless steel piping for reduced pressurization of the different subassemblies on the main manifold.
  •     Borosilicate glass vacuum trap
  •     316L stainless steel vent lines for the different sub-assemblies on the main manifold towards the central suction.
  •     Support frame in 304L stainless steel tubes and aluminum nuts.

     

Instrumentation
 

  •     Condenser cooling water supply equipped with a float flowmeter.
  •     Reactor cooling water supply equipped with a float flowmeter with its control valve.
  •     Measurement of the pressure drop of the column by differential pressure gauge in "U".
  •     Measurements of the supply pressure of the heating steam by manometers.
  •     Flow rate measurement by float flowmeter.
  •     Flow rate measurement by float flowmeter.
  •     Measurement of distillate flow by float flowmeter.
  •     Measurements of reactor pressure by manometers
  •     Control and control cabinet, IP55, equipped with emergency stop, operating buttons and the following interfaces:
  •     Digital temperature indicator of six probes type Pt100 Ω.
Options :
316L stainless steel reduced pressure bag filter capacity 20 liters (cake) + 20 liters (filtrate)
DEMANDER UN DEVIS POUR CETTE MACHINE

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