Your quote (0 machine)
Home > Chemical Processing > Chemical Processing > MP1035

Solid / liquid discontinuous extraction (soxhlet) and discontinuous distillation


Non contractual photo

Service : 230 V / 50 Hz / Single phase: 3 kW.
Cold water 20 ° C / 3 bar: 0 - 6 m3 / h.
Sewer.
Dimensions : 1,80 m x 0,85 m x 2,96 m
Weight : 180kg

Print / download the product sheet
DEMANDER UN DEVIS POUR CETTE MACHINE

Principle of operation

The solid-liquid extraction is a semi-continuous process, coupling distillation with a soxhlet type cartridge containing the solid product impregnated with an active ingredient (solute) to be extracted by dissolution in a hot solvent. The distillation column generates solvent vapors which are condensed; this pure hot solvent feeds the cartridge containing the inert solid and the solute. When the cartridge is full, the solution obtained (solvent and solute) empties automatically by siphoning (leaching) and then returns to the boiler where the solvent is again brought to the boil. The leaching can also be carried out by continuous passage of the solvent or by successive manual draining. The solvent can also be fed in a single "pass" for infusion and the resulting extract is manually withdrawn.




Educational Objectives :
  • Influence of the type of solvent.
  • Influence of the residence time.
  • Influence of the Principle of operation.
  • Study of the hydrodynamics of the column.
  • Study of the separation of a binary or complex solution.
  • Material balance.
  • Calculation of the exchange coefficients of matter.
  • Thermal balances.
  • Determination of the number of theoretical plates (Mc CABE and THIELE, PONCHON and SAVARIT)
  • Determination of the number of transfer units.
Technical specifications :

Equipment
 

  • Boiler made of borosilicate glass, electric heating, equipped with a minimum safety level and maximum temperature safety; useful volume 6 liters.
  • Refrigerant for differential pressure test.
  • Column in borosilicate glass, in two parts with 316L stainless steel lining.
  • Two 316L stainless steel recentering trays, each equipped with a sampling and temperature sampling valve.
  • Borosilicate glass column head, with temperature measurement, equipped with a timer valve to control the reflux ratio.
  • Vertical condenser 316L stainless steel,
  •  316L stainless steel distillate coolant.
  •  Two distillate recipes made of borosilicate glass.
  •  "Soxhlet" extraction cartridge made of borosilicate glass with quick opening and pocket mounted on a 316L stainless steel support.
  •   316L stainless steel connection pipes for the process and reinforced PVC for the cooling fluid.
  •  Support frame in 304L stainless steel tubes and aluminum nuts.
     

Instrumentation
 

  •  Condenser cooling water supply equipped with a float flowmeter with its control valve and a water circulation controller to stop heating due to lack of cooling.
  •  Column pressure drop measurement using a "U" differential pressure gauge.
  •  Control and control cabinet, IP55, equipped with emergency stop, operating buttons and the following interfaces:
  •   Electronic timer controlling the valve of the column head.
  •   Boiler heating control regulator.
  •  Two digital temperature indicators of 7 probes type Pt100 Ω.
DEMANDER UN DEVIS POUR CETTE MACHINE

Other machines associated with the category Chemical Processing
Mini photo-bio-reactor for algae culture
MP46bio
Read more
Pellet granulator mixer
MP411-a
Read more
Laboratory cascading crystallization
MP1002
Read more
Evaporation - discontinuous crystallization
MP1003
Read more
Evaporation - continuous crystallization
MP1004
Read more
Continuous distillation
MP1010
Read more
Continuous distillation
MP1010CR
Read more
Supervised continuous distillation
MP1011
Read more
Supervised continuous distillation
MP1011CR
Read more
Continuous azeotropic distillation
MP1012
Read more
Discontinuous distillation
MP1020
Read more
Discontinuous distillation
MP1020CR
Read more
Flash distillation
MP1025
Read more
Atmospheric dynamic ebulliometry
MP1026
Read more
Fluid-liquid extraction
MP1030
Read more
Supervised liquid-liquid extraction
SP1030
Read more
Fluid-liquid extraction
MP1030CR
Read more
Pulse liquid-liquid extraction
MP1031
Read more
solid / liquid discontinuous extraction (soxhlet)
MP1036
Read more
Absorption / desorption
MP1040
Read more
Absorption / desorption
MP1040CR
Read more
Ascending film evaporator
MP1050
Read more
Double effect ascending film evaporator
MP1052
Read more
Reacted reactor 10 liters
MP1070
Read more
10 liter multi-purpose stirred reactor
MP1071
Read more
laboratory reactor
MP1073-a
Read more
Laboratory reactor
MP1073
Read more
Synthetic unit of synthesis 25 liters
MP1074
Read more
Versatile synthesis unit 50 liters
MP1075
Read more
Reactors stirred - piston
MP1076
Read more
Mixer, decanter, liquid-liquid extraction
MP1032
Read more
Wastewater treatment pilot
MP42-a
Read more